Observation of mechanical fracture and corresponding domain structure changes of polycrystalline PbTiO3 nanotubes

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PbTiO3 (PTO) nanotubes (NTs) were synthesized at various temperatures by gas phase reaction between PbO gas and anatase TiO2 NTs and characterized by piezoresponse force microscopy (PFM). PTO ferroelectric phase was synthesized at as low as 400 degrees C as evidenced by PFM domain images and piezoresponse hysteresis loop measurement. Furthermore, the PTO NTs fabricated at above 500 degrees C underwent mechanical fracture through development of nanocracks due to grain growth, leading to ferroelectric domains with larger size and lower aspect ratio. (C) 2010 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Publisher
WILEY-BLACKWELL
Issue Date
2011-02
Language
English
Article Type
Article
Citation

PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS, v.5, no.2, pp.59 - 61

ISSN
1862-6254
DOI
10.1002/pssr.201004495
URI
http://hdl.handle.net/10203/93590
Appears in Collection
MS-Journal Papers(저널논문)
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