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College of Engineering(공과대학)Dept. of Materials Science and Engineering(신소재공학과)MS-Journal Papers(저널논문)

Synthesis and Characterization of Nano-Sized Epoxy Oligosiloxanes for Fabrication of Transparent Nano Hybrid Materials

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dc.contributor.authorYang, Seung-Cheolko
dc.contributor.authorKim, Jeong-Hwanko
dc.contributor.authorJin, Jung-Hoko
dc.contributor.authorBae, Byeong-Sooko
dc.date.accessioned2009-06-10T08:16:19Z-
dc.date.available2009-06-10T08:16:19Z-
dc.date.created2012-02-06-
dc.date.created2012-02-06-
dc.date.issued2009-04-
dc.identifier.citationJOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS, v.47, no.8, pp.756 - 763-
dc.identifier.issn0887-6266-
dc.identifier.urihttp://hdl.handle.net/10203/9311-
dc.description.abstractNano-sized epoxy oligosiloxanes (EO) were prepared by condensation reaction between 3-glycidoxypropyltrimethoxysilane (GPTS) and Diphenylsilandiol (DPSD). Through a composition change of GPTS and DPSD, EO of various structure and sizes were obtained. The molecular structure and size of EO synthesized were investigated by experimental measurements. Regardless of their composition, molecular structure of EO was linear or branch. The amount of species of high molecular weight and their molecular size increased with addition of DPSD. We confirmed that epoxy groups of EO were thermally cured using a thermal initiator and curing agent. Finally, we fabricated transparent epoxy-based hybrimer films by thermal curing of EO resins. (C) 2009 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 47: 756-763, 2009-
dc.description.sponsorshipThis work was supported by the ERC program of the Korea Science and Engineering Foundation (KOSEF) grant funded by the Korea Ministry of Education, Science and Technology (MEST) (No. R11-2007-04503002-0).en
dc.languageEnglish-
dc.language.isoen_USen
dc.publisherJOHN WILEY & SONS INC-
dc.subjectSOL-GEL PROCESS-
dc.subjectSI-29 NMR-
dc.subjectCOATINGS-
dc.subjectFILMS-
dc.titleSynthesis and Characterization of Nano-Sized Epoxy Oligosiloxanes for Fabrication of Transparent Nano Hybrid Materials-
dc.typeArticle-
dc.identifier.wosid000265263000002-
dc.identifier.scopusid2-s2.0-65649128911-
dc.type.rimsART-
dc.citation.volume47-
dc.citation.issue8-
dc.citation.beginningpage756-
dc.citation.endingpage763-
dc.citation.publicationnameJOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS-
dc.identifier.doi10.1002/polb.21680-
dc.embargo.liftdate9999-12-31-
dc.embargo.terms9999-12-31-
dc.contributor.localauthorBae, Byeong-Soo-
dc.type.journalArticleArticle-
dc.subject.keywordAuthorMALDI-
dc.subject.keywordAuthorneutron scattering-
dc.subject.keywordAuthorNMR-
dc.subject.keywordAuthoroligomer-
dc.subject.keywordPlusSOL-GEL PROCESS-
dc.subject.keywordPlusSI-29 NMR-
dc.subject.keywordPlusCOATINGS-
dc.subject.keywordPlusFILMS-
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