Diels–Alder and Stille Coupling Approach for the Short Protecting-Group-Free Synthesis of Mycophenolic Acid, Its Phenylsulfenyl and Phenylselenyl Analogues, and Reactive Oxygen Species (ROS) Probing Capacity in Water

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A short, protecting-group-free synthesis is achieved. The synthesis is step-efficient and general. A Diets-Alder and Stille cross-coupling approach includes key transformations, allowing for a competitive synthesis which involves a rare halophenol Stille cross coupling study. The phenylselenyl and phenylsulfenyl analogues were prepared as novel compounds in good overall yield. The applicability of one of the intermediates as a potential probe for reactive oxygen species (ROS) in water is investigated.
Publisher
AMER CHEMICAL SOC
Issue Date
2018-06
Language
English
Article Type
Article
Citation

ORGANIC LETTERS, v.20, no.12, pp.3557 - 3561

ISSN
1523-7060
DOI
10.1021/acs.orglett.8b01327
URI
http://hdl.handle.net/10203/244314
Appears in Collection
CH-Journal Papers(저널논문)
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