Facile synthesis of alpha-keto esters via a free radical acylation approach

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dc.contributor.authorKim, Sung Gakko
dc.contributor.authorYoon, JYko
dc.contributor.authorLee, IYko
dc.date.accessioned2013-03-02T16:08:07Z-
dc.date.available2013-03-02T16:08:07Z-
dc.date.created2012-02-06-
dc.date.created2012-02-06-
dc.date.issued1997-05-
dc.identifier.citationSYNLETT, pp.475 - 475-
dc.identifier.issn0936-5214-
dc.identifier.urihttp://hdl.handle.net/10203/74346-
dc.description.abstractA new efficient method for the preparation of alpha-keto esters via a free radical acylation approach using phenylsulfonyl methoxycarbonyl oxime ether 1 has been developed. When an alkyl iodide was treated with 1, hexamethylditin, and acetone in THF at 300 nm for 3 h, alpha-keto ester 3 was obtained in high yield after hydrolysis of the oxime ether 2.-
dc.languageEnglish-
dc.publisherGEORG THIEME VERLAG-
dc.titleFacile synthesis of alpha-keto esters via a free radical acylation approach-
dc.typeArticle-
dc.identifier.wosidA1997XD87200023-
dc.type.rimsART-
dc.citation.beginningpage475-
dc.citation.endingpage475-
dc.citation.publicationnameSYNLETT-
dc.contributor.localauthorKim, Sung Gak-
dc.contributor.nonIdAuthorYoon, JY-
dc.contributor.nonIdAuthorLee, IY-
dc.type.journalArticleArticle-
dc.subject.keywordAuthoralpha-keto esters-
dc.subject.keywordAuthorphenylsulfonyl methoxycarbonyl oxime ether-
dc.subject.keywordAuthorfree radical acylation-
dc.subject.keywordAuthortandem radical reaction-
dc.subject.keywordPlusOMEGA-FORMYLALKYL RADICALS-
dc.subject.keywordPlusCARBON RADICALS-
dc.subject.keywordPlusCYCLIZATION-
dc.subject.keywordPlusKETOESTERS-
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