Facile synthesis of alpha-keto esters via a free radical acylation approach

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A new efficient method for the preparation of alpha-keto esters via a free radical acylation approach using phenylsulfonyl methoxycarbonyl oxime ether 1 has been developed. When an alkyl iodide was treated with 1, hexamethylditin, and acetone in THF at 300 nm for 3 h, alpha-keto ester 3 was obtained in high yield after hydrolysis of the oxime ether 2.
Publisher
GEORG THIEME VERLAG
Issue Date
1997-05
Language
English
Article Type
Article
Citation

SYNLETT, pp.475 - 475

ISSN
0936-5214
URI
http://hdl.handle.net/10203/74346
Appears in Collection
CH-Journal Papers(저널논문)
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