Facile selective detritylation of 5'-primary alcohols of pyrimidine nucleosides using tetra-n-butylammonium peroxydisulfate

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Tetra-n-butylammonium peroxydisulfate has been found to be a good deprotecting reagent for removal of the trityl group: Treatment of 5'-O-dimethoxytrityl uridine or thymidine with tetra-n-butylammonium peroxydisulfate gave the corresponding dedimethoxytritylated nucleosides in excellent yields under neutral and mild conditions and without causing any side reactions such as cleavage of the glycosidic bond. (C) 1997 John Wiley & Sons, Inc.
Publisher
JOHN WILEY & SONS INC
Issue Date
1997
Language
English
Article Type
Article
Keywords

TETRAHYDROFURANYLATION; TETRAHYDROPYRANYLATION; REMOVAL

Citation

HETEROATOM CHEMISTRY, v.8, no.5, pp.435 - 438

ISSN
1042-7163
URI
http://hdl.handle.net/10203/71646
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