Rapid sonochemical synthesis of spherical-shaped mesoporous SBA-15 silica and Ti-incorporated SBA-15 silica materials

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Mesoporous SBA-15 silica materials were synthesized in short time from one hour ultrasonic irradiation, followed by I - 3 h gelation in acidic media. The particle morphology of these sonochemically synthesized mesoporous materials was nearly spherical. Titanium was directly incorporated into SBA-15 silicate framework through sonochemical co-condensation of Ti(O-iPr)(4) and Si(OEt)(4). The Ti-incorporated SBA-15 silica exhibited good catalytic activity for the oxidation of 2,6-di-tert-butylphenol.
Publisher
KOREAN SOC INDUSTRIAL ENGINEERING CHEMISTRY
Issue Date
2003-01
Language
English
Article Type
Article
Keywords

ASYMMETRIC DIETHYLZINC ADDITION; MOLECULAR-SIEVE; TITANIUM; ULTRASOUND; NANOPARTICLES; BENZALDEHYDE; CATALYSIS

Citation

JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY, v.9, no.1, pp.83 - 88

ISSN
1226-086X
URI
http://hdl.handle.net/10203/245147
Appears in Collection
CBE-Journal Papers(저널논문)
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