The structure of MCM-48 determined by electron crystallography

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The structure of the amorphous walls of the mesoporous material MCM-48 was investigated with a combination of high-resolution transmission electron microscopy and selected area electron diffraction, and the three-dimensional structure was reconstructed by electron crystallography. The crystals were well ordered over large areas as shown by the images and diffraction patterns. It was firmly confirmed from Fourier transforms of thin areas that MCM-48 belongs to the Ia3d space group and that the amorphous walls roughly follow the gyroid surface (a minimal surface), but the wall thickness is not uniform.
Publisher
OXFORD UNIV PRESS
Issue Date
1999
Language
English
Article Type
Article; Proceedings Paper
Keywords

MICROSCOPY

Citation

JOURNAL OF ELECTRON MICROSCOPY, v.48, no.6, pp.795 - 798

ISSN
0022-0744
URI
http://hdl.handle.net/10203/12522
Appears in Collection
CH-Journal Papers(저널논문)
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