Preparation of Graphene Liquid Cells for the Observation of Lithium-ion Battery Material

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In this work, we introduce the preparation of graphene liquid cells (GLCs), encapsulating both electrode materials and organic liquid electrolytes between two graphene sheets, and the facile synthesis of one-dimensional nanostructures using electrospinning. The GLC enables in situ transmission electron microscopy (TEM) for the lithiation dynamics of electrode materials. The in situ GLC-TEM using an electron beam for both imaging and lithiation can utilize not only realistic battery electrolytes, but also the high-resolution imaging of various morphological, phase, and interfacial transitions.
Publisher
JOURNAL OF VISUALIZED EXPERIMENTS
Issue Date
2019-02
Language
English
Article Type
Article
Citation

JOVE-JOURNAL OF VISUALIZED EXPERIMENTS, no.144

ISSN
1940-087X
DOI
10.3791/58676
URI
http://hdl.handle.net/10203/251506
Appears in Collection
MS-Journal Papers(저널논문)
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