Production of nitrogen-doped graphite from carbon dioxide using polyaminoborane

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dc.contributor.authorXiong, Ranko
dc.contributor.authorLi, Xueko
dc.contributor.authorByeon, Ayeongko
dc.contributor.authorLee, Jae Wooko
dc.date.accessioned2014-08-29-
dc.date.available2014-08-29-
dc.date.created2013-12-23-
dc.date.created2013-12-23-
dc.date.issued2013-10-
dc.identifier.citationRSC ADVANCES, v.3, no.48, pp.25752 - 25757-
dc.identifier.issn2046-2069-
dc.identifier.urihttp://hdl.handle.net/10203/188637-
dc.description.abstractNitrogen-doped graphite was prepared from gaseous carbon dioxide (CO2) under moderate conditions by polyaminoborane (PAB). This conversion was achieved in a two-step process: CO2 reacted with PAB under mild temperature (<115 degrees C) and low CO2 pressure (<3.10 MPa) to form a solid product containing formate (-OOCH), methoxy (-OCH3), and aliphatic groups; then pyrolysis of this solid product at temperatures up to 750 degrees C under an inert N-2 atmosphere produced a black carbon material. Raman spectroscopic and high-resolution scanning electron microscopic investigations confirmed the multi-layer graphitic structure of this carbon material. Incorporation of nitrogen atoms into the carbon lattice was further detected by X-ray photoelectron spectroscopy (XPS). This work presents the production of nitrogen-doped graphite from gaseous CO2 under mild conditions and provides one feasible option for CO2 capture and conversion at low costs.-
dc.languageEnglish-
dc.publisherROYAL SOC CHEMISTRY-
dc.subjectX-RAY PHOTOELECTRON-
dc.subjectNITRIDE FILMS-
dc.subjectBORON-NITRIDE-
dc.subjectOXYGEN REDUCTION-
dc.subjectAMMONIA BORANE-
dc.subjectPOROUS CARBON-
dc.subjectGRAPHENE-
dc.subjectLITHIUM-
dc.subjectSODIUM-
dc.subjectSPECTROSCOPY-
dc.titleProduction of nitrogen-doped graphite from carbon dioxide using polyaminoborane-
dc.typeArticle-
dc.identifier.wosid000327261700040-
dc.identifier.scopusid2-s2.0-84887979967-
dc.type.rimsART-
dc.citation.volume3-
dc.citation.issue48-
dc.citation.beginningpage25752-
dc.citation.endingpage25757-
dc.citation.publicationnameRSC ADVANCES-
dc.identifier.doi10.1039/c3ra44288h-
dc.embargo.liftdate9999-12-31-
dc.embargo.terms9999-12-31-
dc.contributor.localauthorLee, Jae Woo-
dc.contributor.nonIdAuthorXiong, Ran-
dc.contributor.nonIdAuthorLi, Xue-
dc.contributor.nonIdAuthorByeon, Ayeong-
dc.type.journalArticleArticle-
dc.subject.keywordPlusX-RAY PHOTOELECTRON-
dc.subject.keywordPlusNITRIDE FILMS-
dc.subject.keywordPlusBORON-NITRIDE-
dc.subject.keywordPlusOXYGEN REDUCTION-
dc.subject.keywordPlusAMMONIA BORANE-
dc.subject.keywordPlusPOROUS CARBON-
dc.subject.keywordPlusGRAPHENE-
dc.subject.keywordPlusLITHIUM-
dc.subject.keywordPlusSODIUM-
dc.subject.keywordPlusSPECTROSCOPY-
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